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Simple sublimation apparatus. Water usually cold, is circulated in cold finger to allow the desired compound to be deposited. 1 Cooling water in 2 Cooling water out 3 Vacuum/gas line 4 Sublimation chamber 5 Sublimed compound 6 Crude material 7 External heating
In thermodynamics, the enthalpy of sublimation, or heat of sublimation, is the heat required to sublimate (change from solid to gas) one mole of a substance at a given combination of temperature and pressure, usually standard temperature and pressure (STP). It is equal to the cohesive energy of the solid.
Cold finger used in sublimation.The raw product (6) is in the bottom of the outer tube (4) which is heated (7) while under vacuum (through side-arm 3). The sublimated material collects (5) on the cold finger proper, cooled by a coolant (blue) circulated through ports 1 and 2.
Inadvertently, people who use knives on glass or metal cutting boards are abrading their knife blades. The pressure at the knife edge can easily create microscopic (or even macroscopic) cuts in the board. This cut is a ready source of abrasive material as well as a channel full of this abrasive through which the edge slides.
Los Angeles Times owner Patrick Soon-Shiong, who blocked the newspaper’s endorsement of Kamala Harris and plans to overhaul its editorial board, says he will implement an artificial intelligence ...
In his first term, Trump proposed merging the Department of Education with the Labor Department, but couldn’t get Congress on board. Now his goal is to shutter the department entirely over the ...
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