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Vigreux column in a laboratory setup A laboratory fractionating column is a piece of glassware used to separate vaporized mixtures of liquid compounds with close volatility. Most commonly used is either a Vigreux column or a straight column packed with glass beads or metal pieces such as Raschig rings .
The Snyder column is a wide glass tube divided into sections (usually 3 to 6) by horizontal glass partitions or constrictions. Each partition has a hole, into which seats a hollow glass bead with an inverted "teardrop" shape. Vigreux-like glass "fingers" limit the vertical motion of each bead. [24]
Another example of vapor and liquid contact devices are the spikes in laboratory Vigreux fractionating columns. The trays or plates used in industrial distillation columns are fabricated of circular steel plates and usually installed inside the column at intervals of about 60 to 75 cm (24 to 30 inches) up the height of the column.
There are differences between laboratory-scale and industrial-scale fractionating columns, but the principles are the same. Examples of laboratory-scale fractionating columns (in increasing efficiency) include: Air condenser; Vigreux column (usually laboratory scale only)
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A Raschig ring is a piece of tube, approximately equal in length and diameter, used in large numbers as a packed bed within columns for distillations and other chemical engineering processes. They are usually ceramic, metal, or glass and provide a large surface area within the volume of the column for interaction between liquid and gas vapours.
The Marcusson apparatus, Dean-Stark apparatus, Dean–Stark receiver, distilling trap, or Dean–Stark Head is a piece of laboratory glassware used in synthetic chemistry to collect water [1] [2] (or occasionally other liquid) from a reactor.
Random column packing is the practice of packing a distillation column with randomly fitting filtration material in order to optimize surface area over which reactants can interact while minimizing the complexity of construction of such columns. Random column packing is an alternative to structured column packing.
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