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Porosimetry is an analytical technique used to determine various quantifiable aspects of a material's porous structure, such as pore diameter, total pore volume, surface area, and bulk and absolute densities. The technique involves the intrusion of a non-wetting liquid (often mercury) at high pressure into a material through the use of a ...
In capillary flow porometry, in opposition to mercury intrusion porosimetry, the wetting liquid enters spontaneously the pores of the sample ensuring a total wetting of the material, and therefore the contact angle of the wetting liquid with the sample is 0 and the previous formula can be simplified as: P= 4*γ/D.
[10] [11] This is in effect an "ice intrusion" measurement (c.f. Mercury Intrusion Porosimetry), and as such in part may provide information on pore throat properties. The melting event was then previously expected to provide more accurate information on the pore body.
Mass spectrometry is a scientific technique for measuring the mass-to-charge ratio of ions. It is often coupled to chromatographic techniques such as gas-or liquid chromatography and has found widespread adoption in the fields of analytical chemistry and biochemistry where it can be used to identify and characterize small molecules and proteins ().
The equation first formulated a means to calculate cumulative surface areas of porous solids based on data taken in mercury porosimetry testing. Rootare and Spencer later devised a computer program to carry out automated calculations, "A Computer Program for Pore Volume and Pore Area Distribution," Rootare & Spencer, Perspectives in Powder ...
The Scherrer equation, in X-ray diffraction and crystallography, is a formula that relates the size of sub-micrometre crystallites in a solid to the broadening of a peak in a diffraction pattern. It is often referred to, incorrectly, as a formula for particle size measurement or analysis. It is named after Paul Scherrer.
Porosity or void fraction is a measure of the void (i.e. "empty") spaces in a material, and is a fraction of the volume of voids over the total volume, between 0 and 1, or as a percentage between 0% and 100%.
In the derivation of Washburn's equation, the inertia of the liquid is ignored as negligible. This is apparent in the dependence of length to the square root of time, , which gives an arbitrarily large velocity dL/dt for small values of t.