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A wash bottle is a squeeze bottle with a nozzle, used to rinse various pieces of laboratory glassware, such as test tubes and round bottom flasks. Wash bottles are sealed with a screw-top lid. When hand pressure is applied to the bottle, the liquid inside becomes pressurized and is forced out of the nozzle into a narrow stream of liquid.
A self-pressurising dewar (silver) being filled with liquid nitrogen from a larger storage tank (white). A cryogenic storage dewar (or simply dewar) is a specialised type of vacuum flask used for storing cryogens (such as liquid nitrogen or liquid helium), whose boiling points are much lower than room temperature.
McCartney's bottle or Flat medical bottle: for simultaneous solid and liquid cultures. McIntosh and Filde's anaerobic jar: production of anaerobic conditions for organisms that die in the presence of even little oxygen (anaerobiosis), e.g. tetanus bacteria Microscope: to observe microscopic specimens that cannot be seen by the naked eye ...
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Pressure generally enables faster reactions with cleaner reaction profiles. The above benefits from a pressure reactor has been shown in microwave chemistry. E.g., if a Suzuki Coupling takes 8 hours at 80°C, it only takes 8 minutes at 140°C in a microwave synthesizer. The microwave effect is a controversial topic.
The flask can then be removed from the glove box and taken to a Schlenk line. Once connected to the Schlenk line, the inert gas and/or vacuum can be applied to the flask as required. While the flask is connected to the line under a positive pressure of inert gas, the septum can be replaced with other apparatus, for example a reflux condenser.
Microwave digestion is a chemical technique used to decompose sample material into a solution suitable for quantitative elemental analysis. [1] It is commonly used to prepare samples for analysis using inductively coupled plasma mass spectrometry (ICP-MS) , atomic absorption spectroscopy , and atomic emission spectroscopy (including ICP-AES ).
Vacuum distillation or distillation under reduced pressure is a type of distillation performed under reduced pressure, which allows the purification of compounds not readily distilled at ambient pressures or simply to save time or energy. This technique separates compounds based on differences in their boiling points.