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Crucible steel is steel made by melting pig iron, cast iron, iron, and sometimes steel, often along with sand, glass, ashes, and other fluxes, in a crucible. Crucible steel was first developed in the middle of the 1st millennium BCE in Southern India and Sri Lanka using the wootz process. [1] [2] [3] [4]
A modern crucible used in the production of silicon ingots via the Czochralski process Smaller clay graphite crucibles for copper alloy melting. A crucible is a container in which metals or other substances may be melted or subjected to very high temperatures.
Metal-shaping factories across the country depended on cutting tools made of crucible steel through the 1920s, when electric steel furnaces gained prominence." [ 14 ] Three companies which merged to form Crucible into the largest U.S. crucible-steel-producing company were: [ 10 ] [ 15 ]
In making crucible steel, the blister steel bars were broken into pieces and melted in small crucibles, each containing 20 kg or so. This produced higher quality metal, but increased the cost. The Bessemer process reduced the time needed to make lower-grade steel to about half an hour while requiring only enough coke needed to melt the pig iron.
The flux lowers the melting point of the desired compound, analogous to a wet chemistry recrystallization. [1] The flux is molten in a highly stable crucible that does not react with the flux. Metal crucibles, such as platinum, titanium, and niobium are used for the growth of oxide crystals.
When silicon is grown by the Czochralski method, the melt is contained in a silica crucible. During growth, the walls of the crucible dissolve into the melt and Czochralski silicon therefore contains oxygen at a typical concentration of 10 18 cm −3. Oxygen impurities can have beneficial or detrimental effects.
The process can be carried out in a horizontal or vertical orientation, and usually involves a rotating crucible/ampoule to stir the melt. [ 1 ] The Bridgman method is a popular way of producing certain semiconductor crystals such as gallium arsenide , for which the Czochralski method is more difficult.
Vacuum arc remelting (VAR) is a secondary melting process for production of metal ingots with elevated chemical and mechanical homogeneity for highly demanding applications. [1] The VAR process has revolutionized the specialty traditional metallurgical techniques industry, and has made possible tightly controlled materials used in biomedical ...
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