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A modern crucible used in the production of silicon ingots via the Czochralski process Smaller clay graphite crucibles for copper alloy melting. A crucible is a container in which metals or other substances may be melted or subjected to very high temperatures.
Crucible An evaporating dish is a piece of laboratory glassware used for the evaporation of solutions and supernatant liquids, [ a ] and sometimes to their melting point . Evaporating dishes are used to evaporate excess solvents – most commonly water – to produce a concentrated solution or a solid precipitate of the dissolved substance.
Differential scanning calorimetry (DSC) is a thermoanalytical technique in which the difference in the amount of heat required to increase the temperature of a sample and reference is measured as a function of temperature. [1] Both the sample and reference are maintained at nearly the same temperature throughout the experiment.
A pipeclay triangle is a piece of laboratory apparatus that is used to support a crucible being heated by a Bunsen burner or other heat source. It is made of wires strung in an equilateral triangle on which are strung hollow ceramic, normally fire clay, tubes. The triangle is usually supported on a tripod or iron ring.
A crucible and its lid are pre-weighed after thorough drying. The sample is added to the completely dry crucible and lid and together they are weighed to determine the mass of the sample by difference. The sample is placed in the hot furnace long enough so that complete combustion of the sample occurs. The crucible, lid and ash then are re-weighed.
Since crucible tongs work with the crucible, one must know the safety procedures of the crucible. Before using the crucible, make sure that it is dry; Fill the crucible with sample chemicals to only 1/2 or 2/3, do not fill until it is full; If the user used the crucible to fuse the glass, waiting for the crucible to cool down before cleaning it
It is one of the measurement devices used in the study of thermodynamics, chemistry, and biochemistry. To find the enthalpy change per mole of a substance A in a reaction between two substances A and B, the substances are separately added to a calorimeter and the initial and final temperatures (before the reaction has started and after it has ...
A Gooch crucible, named after Frank Austin Gooch, [1] is a filtration device for laboratory use (and was also called a Gooch filter [2]). It is convenient for collecting a precipitate directly within the vessel in which it is to be dried, possibly ashed , and finally weighed in gravimetric analysis .