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In vacuum applications, a cold trap is a device that condenses all vapors except the permanent gases (hydrogen, oxygen, and nitrogen) into a liquid or solid. [ 2 ] [ needs update ] The most common objective is to prevent vapors being evacuated from an experiment from entering a vacuum pump where they would condense and contaminate it.
A Schlenk line with four ports. The cold trap is on the right. Close-up view, showing the double-oblique stopcock, which allows vacuum (rear line) or inert gas (front line) to be selected. The Schlenk line (also vacuum gas manifold) is a commonly used chemistry apparatus developed by Wilhelm Schlenk. [1] It consists of a dual manifold with ...
The sublimated material collects (5) on the cold finger proper, cooled by a coolant (blue) circulated through ports 1 and 2. A cold finger is a piece of laboratory equipment that is used to generate a localized cold surface. It is named for its resemblance to a finger and is a type of cold trap. The device usually consists of a chamber that a ...
Cold fingers are also used to condense vapors produced by sublimation in which case the result is a solid that adheres to the finger and must be scraped off, or as a cold-trap, where the liquid or solid condensate is not intended to return to the source of the vapor (often used to protect vacuum pumps and/or prevent venting of harmful gasses).
A cooling bath or ice bath, in laboratory chemistry practice, is a liquid mixture which is used to maintain low temperatures, typically between 13 °C and −196 °C. These low temperatures are used to collect liquids after distillation , to remove solvents using a rotary evaporator , or to perform a chemical reaction below room temperature ...
In this function, they are called a cryotrap, waterpump or cold trap, even though the physical mechanism is the same as for a cryopump. Cryotrapping can also refer to a somewhat different effect, where molecules will increase their residence time on a cold surface without actually freezing (supercooling). There is a delay between the molecule ...
The metal clamps on your slow cooker are designed for portability, not cooking. Using them during cooking can cause steam to build up and your device may crack.
Note the white purified camphor on the cold finger, and the dark-brown crude product. Dark green crystals of nickelocene , freshly sublimed on the cold finger of the sublimation apparatus. A typical sublimation apparatus separates a mix of appropriate solid materials in a vessel in which it applies heat under a controllable atmosphere (air ...