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Dry distillation is the heating of solid materials to produce gaseous products (which may condense into liquids or solids). The method may involve pyrolysis or thermolysis, or it may not (for instance, a simple mixture of ice and glass could be separated without breaking any chemical bonds, but organic matter contains a greater diversity of molecules, some of which are likely to break).
Dry distillation (thermolysis and pyrolysis) is the heating of solid materials to produce gases that condense either into fluid products or into solid products. The term dry distillation includes the separation processes of destructive distillation and of chemical cracking, breaking down large hydrocarbon molecules into smaller hydrocarbon ...
A copper retort A glass retort. In a chemistry laboratory, a retort is a device used for distillation or dry distillation of substances. It consists of a spherical vessel with a long downward-pointing neck.
Steam distillation is a separation process that consists of distilling water together with other volatile and non-volatile components. The steam from the boiling water carries the vapor of the volatiles to a condenser ; both are cooled and return to the liquid or solid state, while the non-volatile residues remain behind in the boiling container.
In distillation, a mixture is heated until the more volatile components boil off, the vapors are condensed, and collected in a separate container. In reflux, a reaction involving volatile liquids is carried out at their boiling point, to speed it up; and the vapors that inevitably come off are condensed and returned to the reaction vessel.
A coking factory or a coking plant is where coke and manufactured gas are synthesized from coal using a dry distillation process. The volatile components of the pyrolyzed coal, released by heating to a temperature of between 900°C and 1,400 °C, are generally drawn off and recovered. There are also coking plants where the released components ...
The dry distillation of wood remained the major source of methanol into the early 20th century. [16] Pyrolysis was instrumental in the discovery of many chemical substances, such as phosphorus from ammonium sodium hydrogen phosphate NH 4 NaHPO 4 in concentrated urine, oxygen from mercuric oxide, and various nitrates. [citation needed]
As early as the 1920s, the concept of using hot water and alkali catalysts to produce oil out of biomass was proposed. [6] In 1939, U.S. patent 2,177,557, [7] described a two-stage process in which a mixture of water, wood chips, and calcium hydroxide is heated in the first stage at temperatures in a range of 220 to 360 °C (428 to 680 °F), with the pressure "higher than that of saturated ...
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