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In the paint and coating industries, paint adhesion testing is often used to determine if the paint or coating will adhere properly to the substrates to which they are applied. Several tests measure the resistance of paints and coatings from substrates: cross-cut test, scrape adhesion, pull-off test , and others.
In adhesion tests per ASTM D4541, in which an aluminum stud is bonded to the test surface and the stud is pulled in the direction normal to the surface, both surfaces of the failure interface were analyzed by X-ray photoelectron spectroscopy (XPS). F/C ratio was used as an indicator of the failure mode: F/C of zero corresponds to failure in the ...
A pull-off test, also called stud pull test, is a type of test in which an adhesive connection is made between a stud and a carrier (or object to be tested) by using a glue, possibly an epoxy or polyester resin, that is stronger than the bond that needs to be tested.
Other testing, such as cleavage loading and peel test, can be used to determine both the green strength and final strength of a material. These are typically not reflected on the data sheet for standard adhesives, but can be used for testing of adhesives based on their applications in residential and commercial environments.
Accelerated testing may induce reaction kinetics that is not applicable to the actual service environment of an adhesive, which could cause greater concern than is necessary for certain adhesives. High temperatures are often avoided because it frequently causes new reactions to occur.
For example, ASTM D1000 has test methods for electrical tapes. There are ASTM specifications for many tapes including D2301 for vinyl electrical tape, D5486 for box-sealing tape, etc. Several of the ASTM test methods are coordinated with PSTC, other trade associations, and other international organizations.
After degreasing, a good test to determine cleanliness of the surface is to use a drop of water. If the drop spreads on the surface, a low contact angle and good wettability has been achieved, which indicates the surface is clean and ready for application of the adhesive. If the drop beads up or retains its shape, the degreasing process should ...
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