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In analytical chemistry, sample preparation (working-up) refers to the ways in which a sample is treated prior to its analyses. Preparation is a very important step in most analytical techniques, because the techniques are often not responsive to the analyte in its in-situ form, or the results are distorted by interfering species.
Sample preparation for mass spectrometry is used for the optimization of a sample for analysis in a mass spectrometer (MS). Each ionization method has certain factors that must be considered for that method to be successful, such as volume, concentration , sample phase, and composition of the analyte solution.
Microwave digestion is a chemical technique used to decompose sample material into a solution suitable for quantitative elemental analysis. [1] It is commonly used to prepare samples for analysis using inductively coupled plasma mass spectrometry (ICP-MS), atomic absorption spectroscopy, and atomic emission spectroscopy (including ICP-AES).
A normal experiment may involve 1–10 mL solution with an analyte concentration between 1 and 10 mmol/L. More advanced voltammetric techniques can work with microliter volumes and down to nanomolar concentrations. Chemically modified electrodes are employed for the analysis of organic and inorganic samples.
A riffle box is a box containing a number (between 3 and 12) of "chutes" - slotted paths through which particles of the sample may slide. The sample is dropped into the top, and the box produces two equally divided subsamples. Riffle boxes are commonly used in mining to reduce the size of crushed rock samples prior to assaying.
The method uses headspace gas injected into a gas chromatographic column (GC) to determine the original concentration in a water sample. [9] A sample of water is collected in the field in a vial without headspace and capped with a Teflon septum or crimp top to minimize the escape of volatile gases. It is beneficial to store the bottles upside ...
SPE is in fact a method of chromatography, in the sense of having a mobile phase, carrying mixtures through a stationary phase, packed inside a column.The chromatographic process is harnessed to create a solid-liquid extractive technique—allowing separation of a mixture of components by taking advantage of large differences between the solid and liquid phase K eq, or equilibrium constant ...
An oscillating force is applied to a polymer sample and the sample’s response is recorded. DMA documents the lag between force applied and deformation recovery in the sample. Viscoelastic samples exhibit a sinusoidal modulus called the dynamic modulus. Both energy recovered and lost are considered during each deformation and described ...