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The Trapp mixture is a specific mixture of organic solvents that allows chemical reactions to take place at very low temperatures. [1] It is made up of THF:diethyl ether:pentane in a 4:4:1 ratio which remains liquid down to −110 °C and the same solvents in a 4:1:1 ratio remain a liquid down to −120 °C.
Some workers prefer the opposite arrangement, where vapors flow down the wall of the trap, and are sucked up the inner tube; this reduces blockage. [1] In vacuum applications, a cold trap is a device that condenses all vapors except the permanent gases (hydrogen, oxygen, and nitrogen) into a liquid or solid.
Organic solvent or salt Temp (°C) Dry ice p-xylene +13 Dry ice Dioxane +12 Dry ice Cyclohexane +6 Dry ice Benzene +5 Dry ice Formamide +2 Ice Salts (see: left) 0 to −40 Liquid N 2: Cycloheptane −12 Dry ice Benzyl alcohol −15 Dry ice Tetrachloroethylene −22 Dry ice Carbon tetrachloride −23 Dry ice 1,3-Dichlorobenzene −25 Dry ice o ...
The inert-gas line is vented through an oil bubbler, while solvent vapors and gaseous reaction products are prevented from contaminating the vacuum pump by a liquid-nitrogen or dry-ice/acetone cold trap. Special stopcocks or Teflon taps allow vacuum or inert gas to be selected without the need for placing the sample on a separate line. [3]
A sewer pipe is normally at neutral air pressure compared to the surrounding atmosphere.When a column of waste water flows through a pipe, it compresses air ahead of it in the system, creating a positive pressure that must be released so it does not push back on the waste stream and downstream traps, slow drainage, and induce potential clogs.
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