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When heated over a flame, the crucible is often held inside a pipeclay triangle which itself is held on top of a tripod. Crucibles and their covers are made of heat-resistant materials, usually porcelain, alumina or an inert metal. One of the earliest uses of platinum was to make crucibles.
Crucible An evaporating dish is a piece of laboratory glassware used for the evaporation of solutions and supernatant liquids, [ a ] and sometimes to their melting point . Evaporating dishes are used to evaporate excess solvents – most commonly water – to produce a concentrated solution or a solid precipitate of the dissolved substance.
Since crucible tongs work with the crucible, one must know the safety procedures of the crucible. Before using the crucible, make sure that it is dry; Fill the crucible with sample chemicals to only 1/2 or 2/3, do not fill until it is full; If the user used the crucible to fuse the glass, waiting for the crucible to cool down before cleaning it
A pipeclay triangle is a piece of laboratory apparatus that is used to support a crucible being heated by a Bunsen burner or other heat source. It is made of wires strung in an equilateral triangle on which are strung hollow ceramic, normally fire clay, tubes. The triangle is usually supported on a tripod or iron ring.
A crucible and its lid are pre-weighed after thorough drying. The sample is added to the completely dry crucible and lid and together they are weighed to determine the mass of the sample by difference. The sample is placed in the hot furnace long enough so that complete combustion of the sample occurs. The crucible, lid and ash then are re-weighed.
A watch glass is a circular concave piece of glass used in chemistry as a surface to evaporate a liquid, to hold solids while being weighed, for heating a small amount of substance, and as a cover for a beaker. When used to cover beakers, the purpose is generally to prevent dust or other particles from entering the beaker; the watch glass does ...
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The flux lowers the melting point of the desired compound, analogous to a wet chemistry recrystallization. [1] The flux is molten in a highly stable crucible that does not react with the flux. Metal crucibles, such as platinum , titanium , and niobium are used for the growth of oxide crystals.
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