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In analytical chemistry, sample preparation (working-up) refers to the ways in which a sample is treated prior to its analyses. Preparation is a very important step in most analytical techniques, because the techniques are often not responsive to the analyte in its in-situ form, or the results are distorted by interfering species .
Atomic absorption spectroscopy (AAS) is a spectro-analytical procedure for the quantitative measurement of chemical elements. AAS is based on the absorption of light by free metallic ions that have been atomized from a sample. An alternative technique is atomic emission spectroscopy (AES).
When working with limiting amount of sample, an analyst might need to make a single addition, but it is generally considered a best practice to make at least two additions whenever possible. [5] Note that this is not limited to liquid samples. In atomic absorption spectroscopy, for example, standard additions are often used with solid as the ...
Elemental analysis is a process where a sample of some material (e.g., soil, waste or drinking water, bodily fluids, minerals, chemical compounds) is analyzed for its elemental and sometimes isotopic composition.
This is especially important for solid samples where there is a strong matrix influence. [5] In cases with complex or unknown matrices, the standard addition method can be used. [3] In this technique, the response of the sample is measured and recorded, for example, using an electrode selective for the analyte.
The gravimetric analysis involves determining the amount of material present by weighing the sample before and/or after some transformation. A common example used in undergraduate education is the determination of the amount of water in a hydrate by heating the sample to remove the water such that the difference in weight is due to the loss of ...
A list of chemical analysis methods with acronyms. A. Atomic absorption spectroscopy (AAS) Atomic emission spectroscopy (AES) Atomic ... 3 languages ...
The sample is vaporized in the heated graphite tube; the amount of light energy absorbed in the vapor is proportional to atomic concentrations. Analysis of each sample takes from 1 to 5 minutes, and the results for a sample is the average of triplicate analysis.