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Vapour-liquid equilibrium of 2-propanol/water showing positive azeotropic behaviour. An azeotrope (/ ə ˈ z iː ə ˌ t r oʊ p /) [1] or a constant heating point mixture is a mixture of two or more liquids whose proportions cannot be changed by simple distillation. [2]
In organic chemistry, some dehydration reactions are subject to unfavorable but fast equilibria. One example is the formation of dioxolanes from aldehydes: [9] RCHO + (CH 2 OH) 2 RCH(OCH 2) 2 + H 2 O. Such unfavorable reactions proceed when water is removed by azeotropic distillation.
Dimethylformamide, DMF is an organic compound with the chemical formula H C O N(CH 3) 2.Its structure is HC(=O)−N(−CH 3) 2.Commonly abbreviated as DMF (although this initialism is sometimes used for dimethylfuran, or dimethyl fumarate), this colourless liquid is miscible with water and the majority of organic liquids.
This Wikipedia page provides a comprehensive list of boiling and freezing points for various solvents.
Dimethylacetamide (DMAc or DMA) is the organic compound with the formula CH 3 C(O)N(CH 3) 2. This colorless, water-miscible, high-boiling liquid is commonly used as a polar solvent in organic synthesis. DMA is miscible with most other solvents, although it is poorly soluble in aliphatic hydrocarbons.
In chemistry, a dehydration reaction is a chemical reaction that involves the loss of water from the reacting molecule or ion. Dehydration reactions are common processes, the reverse of a hydration reaction .
Figure 2: Simplified animation of a typical dry vacuum distillation column as used in oil refineries Figure 3: Large-scale vacuum distillation tower at the Fawley oil refinery [9] Industrial-scale vacuum distillation [10] has several advantages. Close boiling mixtures may require many equilibrium stages to separate the key components.
From the solution crystallizes the sesquihydrate K 2 CO 3 ·1.5H 2 O ("potash hydrate"). Heating this solid above 200 °C (392 °F) gives the anhydrous salt. In an alternative method, potassium chloride is treated with carbon dioxide in the presence of an organic amine to give potassium bicarbonate, which is then calcined: 2 KHCO 3 → K 2 CO 3 ...