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A Thiele tube can be used to measure the boiling point of a liquid by the Siwoloboff method. A sample in a fusion tube is attached to a thermometer with a rubber band, and immersed in the tube. A sealed capillary, open end pointing down, is placed in the fusion tube. The Thiele tube is heated; dissolved gases evolve from the sample first.
A boiling tube is a large test tube intended specifically for boiling liquids. A test tube filled with water and upturned into a water-filled beaker is often used to capture gases, e.g. in electrolysis demonstrations. A test tube with a stopper is often used for temporary storage of chemical or biological samples.
These tubes are usually made of glass, but can also be made of plastic or metal. They vary in size and purpose. Laboratory sample tubes must not be confused with glass tubing, which can be utilized to carry fluid between laboratory equipment. Example laboratory sample tubes are listed below: Ignition tube; Test tube; Boiling tube; NMR tube
The Siwoloboff method is used to determine the boiling point of small samples of liquid chemicals. A sample in an ignition tube (also called a fusion tube) is attached to a thermometer with a rubber band, and immersed in a Thiele tube, water bath, or other suitable medium for heating. A sealed capillary, open end pointing down, is placed in the ...
While the outward designs of apparatuses can vary greatly, most apparatuses use a sample loaded into a sealed capillary tube (melting-point tube), which is then placed in the apparatus. The sample is then heated, either by a heating block or an oil bath, and as the temperature increases, the sample is observed to determine when the phase change ...
Round-bottom flasks are often used to contain chemical reactions run by chemists, especially for reflux set-ups and laboratory-scale synthesis. [3] Boiling chips are added in distilling flasks for distillations or boiling chemical reactions to allow a nucleation site for gradual boiling. This nucleation avoids a sudden boiling surge where the ...
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The simplest type of condenser is a straight tube, cooled only by the surrounding air. The tube is held in a vertical or oblique position, and the vapor is fed through the upper end. The heat of condensation is carried away by convection. The neck of the retort is a classical example of a straight tube condenser.