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Gas chromatography-mass spectrometry is a widely used analytical technique for the detection of volatile compounds. Ionization techniques most frequently used in forensic toxicology include electron ionization (EI) or chemical ionization (CI), with EI being preferred in forensic analysis due to its detailed mass spectra and its large library of ...
[23] [24] The coupling of a gas chromatograph with a mass spectrometer allowed for the identification of a wide range of substances. [24] GC-MS analysis is widely considered the "gold standard" for forensic analysis due to its sensitivity and versatility along with its ability to quantify the amount of substance present. [25]
Flow injection analysis (FIA) Fourier transform infrared spectroscopy (FTIR) G. Gas chromatography (GC) Gas chromatography-mass spectrometry (GC-MS)
For the analysis of volatile compounds, a purge and trap (P&T) concentrator system may be used to introduce samples. The target analytes are extracted by mixing the sample with water and purge with inert gas (e.g. Nitrogen gas) into an airtight chamber, this is known as purging or sparging.
One of the most widely used methods for headspace analysis is described by the United States Environmental Protection Agency (USEPA). Originally developed by the R.S. Kerr USEPA Laboratory in Ada, Oklahoma as a "high quality, defendable, and documented way to measure" methane, ethane, and ethene, [7] [8] RSKSOP-175 is a standard operating procedure (SOP) and an unofficial method employed by ...
Post-mortem diagnosis is the use of post-mortem chemistry analysis tests to diagnose a disease after someone has died. Some diseases are unknown until death, or were not correctly diagnosed earlier. One way that diseases can be diagnosed is by examining the concentrations of certain substances in the blood or other sample types.
For instance, Arizona, which has an average electricity rate of 42.10 cents per kilowatt-hour, or 14.7% below the national average of 16.63 cents, still has the second highest average monthly bill ...
Gravimetric analysis describes a set of methods used in analytical chemistry for the quantitative determination of an analyte (the ion being analyzed) based on its mass. The principle of this type of analysis is that once an ion's mass has been determined as a unique compound, that known measurement can then be used to determine the same analyte's mass in a mixture, as long as the relative ...