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Usually X-ray diffraction in spectrometers is achieved on crystals, but in Grating spectrometers, the X-rays emerging from a sample must pass a source-defining slit, then optical elements (mirrors and/or gratings) disperse them by diffraction according to their wavelength and, finally, a detector is placed at their focal points.
X-ray diffraction is a generic term for phenomena associated with changes in the direction of X-ray beams due to interactions with the electrons around atoms. It occurs due to elastic scattering , when there is no change in the energy of the waves.
Laser spectroscopy is a spectroscopic technique that uses lasers to be able determine the emitted frequencies of matter. [87] The laser was invented because spectroscopists took the concept of its predecessor, the maser, and applied it to the visible and infrared ranges of light. [87]
He continued his work on X-rays with much success. He invented the X-ray spectrometer and with his son, Lawrence Bragg, then a research student at Cambridge, founded the new science of X-ray crystallography, the analysis of crystal structure using X-ray diffraction. [20]
An intuitive understanding of X-ray diffraction can be obtained from the Bragg model of diffraction. In this model, a given reflection is associated with a set of evenly spaced sheets running through the crystal, usually passing through the centers of the atoms of the crystal lattice.
In 1913, Moseley observed and measured the X-ray spectra of various chemical elements (mostly metals) that were found by the method of diffraction through crystals. [14] This was a pioneering use of the method of X-ray spectroscopy in physics, using Bragg's diffraction law to determine the X-ray wavelengths.
An X-ray diffraction pattern of a crystallized enzyme. The pattern of spots (reflections) and the relative strength of each spot (intensities) can be used to determine the structure of the enzyme. The relative intensities of the reflections provides information to determine the arrangement of molecules within the crystal in atomic detail.
Portrait of William Lawrence Bragg taken when he was around 40 years old. Sir William Lawrence Bragg (31 March 1890 – 1 July 1971), known as Lawrence Bragg, was an Australian-born British physicist and X-ray crystallographer, discoverer (1912) of Bragg's law of X-ray diffraction, which is basic for the determination of crystal structure.