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The parent isoindole was prepared by flash vacuum pyrolysis of an N-substituted isoindoline. [5] N-Substituted isoindoles, which are easier to handle, can be prepared by dehydration of isoindoline-N-oxides. They also arise by myriad other methods, e.g., starting from xylylene dibromide (C 6 H 4 (CH 2 Br) 2).
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The page provides a comprehensive list of isomers of dodecane, including their chemical structures and properties.
2,5-Dimethoxy-4-iodoamphetamine (DOI) is a psychedelic drug and a substituted amphetamine. Unlike many other substituted amphetamines, however, it is not primarily a stimulant . [ 3 ] DOI has a stereocenter and R -(−)-DOI is the more active stereoisomer .
[3] The preparation of 1,1-diiodoethane from gem-dihaloalkanes [3] To be specific, mix 0.4 mol (~39.6 g) of 1,1-dichloroethane with 1.2 mol (~187 g) of ethyl iodide, and ~2.0 g of aluminium chloride. Heat for three hours using steam bath. Then, wash the mixture with H 2 O and NaHSO 3 respectively, and dry with MgSO 4. By boiling at 76-76 °C ...
Diiodomethane is a reagent for installing the CH 2 group. In the Simmons–Smith reaction, it is a source of methylene. [4] In fact the Simmons–Smith reaction does not produce free carbene but proceeds via Zn-CH 2 I intermediates. Diiodomethane is also a source of the equivalent of CH 2+ 2. The synthesis of Fe 2 (CH 2)(CO) 8 illustrates this ...
Hagemann's ester, ethyl 2-methyl-4-oxo-2-cyclohexenecarboxylate, is an organic compound that was first prepared and described in 1893 by German chemist Carl Hagemann. The compound is used in organic chemistry as a reagent in the synthesis of many natural products including sterols , trisporic acids , and terpenoids .
1.624 g/mL Boiling point: 180 °C (356 °F; 453 K) Solubility in water. Insoluble Hazards Flash point: 71 °C (160 °F; 344 K) Related compounds Related compounds.