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This page contains tables of azeotrope data for various binary and ternary mixtures of solvents. The data include the composition of a mixture by weight (in binary azeotropes, when only one fraction is given, it is the fraction of the second component), the boiling point (b.p.) of a component, the boiling point of a mixture, and the specific gravity of the mixture.
Ethylmagnesium bromide is commercially available, usually as a solution in diethyl ether or tetrahydrofuran. It may be prepared in the normal manner of Grignard reagents — by reacting bromoethane with magnesium in diethyl ether : [ 2 ]
Substance Formula 0 °C 10 °C 20 °C 30 °C 40 °C 50 °C 60 °C 70 °C 80 °C 90 °C 100 °C Barium acetate: Ba(C 2 H 3 O 2) 2: 58.8: 62: 72: 75: 78.5: 77: 75
The following chart shows the solubility of various ionic compounds in water at 1 atm pressure and room temperature (approx. 25 °C, 298.15 K). "Soluble" means the ionic compound doesn't precipitate, while "slightly soluble" and "insoluble" mean that a solid will precipitate; "slightly soluble" compounds like calcium sulfate may require heat to precipitate.
The use of 1,2-dibromoethane is advantageous as its action can be monitored by the observation of bubbles of ethylene. Furthermore, the side-products are innocuous: Mg + BrC 2 H 4 Br → C 2 H 4 + MgBr 2. The amount of Mg consumed by these activating agents is usually insignificant.
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2 CH 3 MgX + 2 dioxane ⇌ (CH 3) 2 Mg + MgX 2 (μ-dioxane) 2 ↓. In such procedures, the dimethylmagnesium exists as the ether adduct, not the polymer. [4] Addition of 1,4-dioxane causes precipitation of solid MgX 2 (μ-dioxane) 2, a coordination polymer. [4] This precipitation drives the Schlenk equilibrium toward (CH 3) 2 Mg. Related ...
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