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An Automatic Oil Muffle Furnace, circa 1910. Petroleum is contained in tank A, and is kept under pressure by pumping at intervals with the wooden handle, so that when the valve B is opened, the oil is vaporized by passing through a heating coil at the furnace entrance, and when ignited burns fiercely as a gas flame.
A 19th-century assay laboratory in Tombstone Courthouse State Historic Park, Arizona. A model of a late 19th-century Canadian seal used to certify the quality of assayed gold. A metallurgical assay is a compositional analysis of an ore, metal, or alloy, usually performed in order to test for purity or quality.
The use of microwave energy allows for fast sample heating, reducing digestion time to as little as one hour. Another common means to decompose samples for elemental analysis is dry-ashing, in which samples are incinerated in a muffle furnace. [2] The resultant ash is then dissolved for analysis, usually into dilute nitric acid.
A crucible and its lid are pre-weighed after thorough drying. The sample is added to the completely dry crucible and lid and together they are weighed to determine the mass of the sample by difference. The sample is placed in the hot furnace long enough so that complete combustion of the sample occurs. The crucible, lid and ash then are re-weighed.
Bunsen sought to improve existing laboratory burner lamps as regards economy, simplicity, and flame temperature, and adapt them to coal-gas fuel. While the building was under construction in late 1854, Bunsen suggested certain design principles to the university's mechanic, Peter Desaga , and asked him to construct a prototype.
A 'muffle' is the incineration chamber where the body is put. In order to improve the speed at which bodies burned, the muffles were internally joined, resulting in the ashes of individual bodies being mixed. This was illegal, but all subsequent multi-muffle ovens built for the concentration camps were designed in the same way.
Molybdenum disilicide heating elements can be used for temperatures up to 1800 °C, in electric furnaces used in laboratory and production environment in production of glass, steel, electronics, ceramics, and in heat treatment of materials. While the elements are brittle, they can operate at high power without aging, and their electrical ...
Gravimetric analysis describes a set of methods used in analytical chemistry for the quantitative determination of an analyte (the ion being analyzed) based on its mass. The principle of this type of analysis is that once an ion's mass has been determined as a unique compound, that known measurement can then be used to determine the same analyte's mass in a mixture, as long as the relative ...
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