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Potassium perchlorate in crystal form. Potassium perchlorate is prepared industrially by treating an aqueous solution of sodium perchlorate with potassium chloride.This single precipitation reaction exploits the low solubility of KClO 4, which is about 1/100 as much as the solubility of NaClO 4 (209.6 g/100 mL at 25 °C).
Hodgdon also makes "Triple Seven", a sulfur-free black powder substitute containing potassium perchlorate and 3-Nitrobenzoic acid, and "Black Mag3". [10] These are both more energetic by mass than black powder and can produce higher velocities and pressures.
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The stoichiometric ratio is 34.2% aluminum and 65.8% perchlorate by mass. A ratio of seven parts potassium perchlorate to three parts dark pyro aluminium is the composition used by most pyrotechnicians. For best results, the aluminium powder should be "Dark Pyro" grade, with a flake particle shape, and a particle size of fewer than 10 micrometres.
In contact with potassium nitrate (e.g. in black powder) produces potassium perchlorate and hygroscopic ammonium nitrate; no such reaction with sodium nitrate. Reacts with potassium chlorate, producing unstable, gradually decomposing ammonium chlorate; such combination has to be avoided. [1] Nitronium perchlorate
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With further heating, potassium perchlorate decomposes to potassium chloride and oxygen: KClO 4 → KCl + 2 O 2. The safe performance of this reaction requires very pure reagents and careful temperature control. Molten potassium chlorate is an extremely powerful oxidizer and spontaneously reacts with many common materials such as sugar.