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Dry distillation is the heating of solid materials to produce gaseous products (which may condense into liquids or solids). The method may involve pyrolysis or thermolysis, or it may not (for instance, a simple mixture of ice and glass could be separated without breaking any chemical bonds, but organic matter contains a greater diversity of molecules, some of which are likely to break).
Dry distillation (thermolysis and pyrolysis) is the heating of solid materials to produce gases that condense either into fluid products or into solid products. The term dry distillation includes the separation processes of destructive distillation and of chemical cracking, breaking down large hydrocarbon molecules into smaller hydrocarbon ...
A McCabe–Thiele diagram for the distillation of a binary (two-component) feed is constructed using the vapor-liquid equilibrium (VLE) data—which is how vapor is concentrated when in contact with its liquid form—for the component with the lower boiling point. Figure 1: Typical McCabe–Thiele diagram for distillation of a binary feed
A process of heating oil shale to produce shale oil, oil shale gas, and spent shale is commonly called retorting. Airtight vessels to apply pressure as well as heat are called autoclaves . In the food industry , pressure cookers are often referred to as "retorts", meaning " canning retorts" for sterilization under high temperature (116–130 °C).
The dry distillation of wood remained the major source of methanol into the early 20th century. [16] Pyrolysis was instrumental in the discovery of many chemical substances, such as phosphorus from ammonium sodium hydrogen phosphate NH 4 NaHPO 4 in concentrated urine , oxygen from mercuric oxide , and various nitrates .
Aspen Plus, Aspen HYSYS, ChemCad and MATLAB, PRO are the commonly used process simulators for modeling, simulation and optimization of a distillation process in the chemical industries. [ 1 ] [ 2 ] Distillation is the technique of preferential separation of the more volatile components from the less volatile ones in a feed followed by ...
Phase diagram (left) and process flow diagram (right) of an apparatus for the azeotropic distillation with "material separation agent". In this case the phase diagram includes a zone where components are not miscible, so following the condensation of the azeotrope, it is possible to separate the liquid components through decantation.
Extractive distillation is defined as distillation in the presence of a miscible, high-boiling, relatively non-volatile component, the solvent, that forms no azeotrope with the other components in the mixture. The method is used for mixtures having a low value of relative volatility, nearing unity. Such mixtures cannot be separated by simple ...