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Dry ice: Acetonitrile-41 Dry ice: Pyridine-42 Dry ice: Cyclohexanone-46 Dry ice: m-Xylene-47 Dry ice: Diethyl carbitol-52 Dry ice: n-Octane-56 Dry ice: Diisopropyl ether-60 Dry ice: Chloroform-61 Liquid N 2: Chloroform-63 [2] Dry ice: Ethanol-72 Note: without the addition of ethylene glycol, temp is -78 °C. Dry ice: Trichloroethylene-73 Dry ...
Cooling bath. A typical experimental setup for an aldol reaction. Both flasks are submerged in a dry ice/acetone cooling bath (−78 °C) the temperature of which is being monitored by a thermocouple (the wire on the left). A cooling bath or ice bath, in laboratory chemistry practice, is a liquid mixture which is used to maintain low ...
Vapour may also be ignited by the static electricity which can build up when ether is being poured from one vessel into another. The autoignition temperature of diethyl ether is 160 °C (320 °F). The diffusion of diethyl ether in air is 9.18 × 10 −6 m 2 /s (298 K, 101.325 kPa). [citation needed]
Cold bath: While a soak in a cold-water bath can also be useful, Dr. Kutcher says that it’s more difficult to keep the temperature consistent than it is in a cold shower.
The order of addition of the reagents of the Mitsunobu reaction can be important. Typically, one dissolves the alcohol, the carboxylic acid, and triphenylphosphine in tetrahydrofuran or other suitable solvent (e.g. diethyl ether), cool to 0 °C using an ice-bath, slowly add the DEAD dissolved in THF, then stir at room temperature for several hours.
Dry ice colloquially means the solid form of carbon dioxide. It is commonly used for temporary refrigeration as CO 2 does not have a liquid state at normal atmospheric pressure and sublimes directly from the solid state to the gas state. It is used primarily as a cooling agent, but is also used in fog machines at theatres for dramatic effects.
When dry ice was mixed with diethyl ether, it was called "Thilorier's mixture", [36] [37] presumably since Thilorier had noted in 1835 that a mixture of liquid carbon dioxide and ether produced extreme cold when sprayed on objects. [38] It was subsequently found that under reduced pressure, temperatures as low as −110 °C could be maintained ...
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...