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Air-free techniques refer to a range of manipulations in the chemistry laboratory for the handling of compounds that are air-sensitive. These techniques prevent the compounds from reacting with components of air, usually water and oxygen; less commonly carbon dioxide and nitrogen. A common theme among these techniques is the use of a fine (10 0 ...
Air from the tip rises to fill the space left vacant, and the tip air is then replaced by the liquid, which is drawn up into the tip and thus available for transport and dispensing elsewhere. When the pipette knob is pressed on an air displacement pipette, the piston inside the instrument moves down to let air out. Air is displaced by the piston.
Septa seal the two conical flasks. A cannula is used to transfer THF from the flask on the right to the flask on the left.. Cannula transfer or cannulation is a set of air-free techniques used with a Schlenk line, in transferring liquid or solution samples between reaction vessels via cannulae, avoiding atmospheric contamination.
Reverse pipetting is a technique to dispense a measured quantity of liquid by means of air displacement pipette.The technique is mainly recommended for solutions with a high viscosity or a tendency to foam: [1] as it reduces the risk of splashing, foam or bubble formation.
The liquid dispensed by the pipette. Corrosive and volatile liquids tend to emit vapors which ascend into the pipette shaft even under proper operating conditions and may corrode the metal piston and springs, or the seals and o-rings that provide an air-tight seal between the piston and the surrounding sleeve. Proper and careful handling.
The air bursts modify the air pressure and flow, and change the boundaries between streams of air moving at different speeds. The company built a 25% scale prototype with 11 conventional control surfaces, as well as 14 banks fed by eight air channels. [3] In 2023, the aircraft received its official designation as X-65. [4]
Mixing of liquids occurs frequently in process engineering. The nature of liquids to blend determines the equipment used. Single-phase blending tends to involve low-shear, high-flow mixers to cause liquid engulfment, while multi-phase mixing generally requires the use of high-shear, low-flow mixers to create droplets of one liquid in laminar, turbulent or transitional flow regimes, depending ...
Positive displacement pipettes are a type of pipette that operates via piston-driven displacement. [1] [2] Unlike an air displacement pipette, which dispenses liquid using an air cushion in the pipette tip, the piston in a positive displacement pipette makes direct contact with the sample, allowing the aspiration force to remain constant.
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