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  2. Work-up - Wikipedia

    en.wikipedia.org/wiki/Work-up

    separating the reaction mixture into organic and aqueous layers by liquid-liquid extraction. removal of solvents by evaporation. purification by chromatography, distillation or recrystallization. The work-up steps required for a given chemical reaction may require one or more of these manipulations.

  3. McMurry reaction - Wikipedia

    en.wikipedia.org/wiki/McMurry_reaction

    The McMurry reaction of benzophenone. The McMurry reaction is an organic reaction in which two ketone or aldehyde groups are coupled to form an alkene using a titanium chloride compound such as titanium(III) chloride and a reducing agent.

  4. Hoesch reaction - Wikipedia

    en.wikipedia.org/wiki/Hoesch_reaction

    The mechanism of the reaction involves two steps. The first step is a nucleophilic addition to the nitrile with the aid of a polarizing Lewis acid, forming an imine, which is later hydrolyzed during the aqueous workup to yield the final aryl ketone. Hoesch reaction mechanism

  5. Acid–base extraction - Wikipedia

    en.wikipedia.org/wiki/Acid–base_extraction

    Acid–base extraction is a subclass of liquid–liquid extractions and involves the separation of chemical species from other acidic or basic compounds. [1] It is typically performed during the work-up step following a chemical synthesis to purify crude compounds [2] and results in the product being largely free of acidic or basic impurities.

  6. Reductions with samarium(II) iodide - Wikipedia

    en.wikipedia.org/wiki/Reductions_with_samarium...

    Workup procedures may vary depending on the stability of the products. If the organic products of the reaction are stable to aqueous acid, aqueous hydrochloric acid may be used to quench the reaction. For workups involving acid-labile products, mildly basic solutions or pH 7–8 buffers may be used.

  7. Corey–House synthesis - Wikipedia

    en.wikipedia.org/wiki/Corey–House_synthesis

    The scope of the Corey-House synthesis is exceptionally broad, and a range of lithium diorganylcuprates (R 2 CuLi, R = 1°, 2°, or 3° alkyl, aryl, or alkenyl) and organyl (pseudo)halides (RX, R = methyl, benzylic, allylic, 1°, or cyclic 2° alkyl, aryl, or alkenyl and X = Br, I, OTs, or OTf; X = Cl is marginal) will undergo coupling as the nucleophilic and electrophilic coupling partners ...

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  9. Workup - Wikipedia

    en.wikipedia.org/wiki/Workup

    Workup may refer to: Workup (chemistry) , manipulations carried out after the main chemical reaction to secure the desired product Workup, a game of practice baseball (see scrub baseball )