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Di-tert-butyl dicarbonate is a reagent widely used in organic synthesis. [1] Since this compound can be regarded formally as the acid anhydride derived from a tert-butoxycarbonyl (Boc) group, it is commonly referred to as Boc anhydride. This pyrocarbonate reacts with amines to give N-tert-butoxycarbonyl or so-called Boc
This page contains tables of azeotrope data for various binary and ternary mixtures of solvents. The data include the composition of a mixture by weight (in binary azeotropes, when only one fraction is given, it is the fraction of the second component), the boiling point (b.p.) of a component, the boiling point of a mixture, and the specific gravity of the mixture.
Add the amine to sodium hydroxide and di-tert-butyl dicarbonate in water and THF at 0 °C then warm to ambient temperature. [13] Heating a mixture of the amine to be protected and di-tert-butyl dicarbonate in a biphasic mixture of chloroform and aqueous sodium bicarbonate at reflux for 90 minutes. [14]
Density: 1.101 g/mL at 25 °C ... Di-tert-butyl dicarbonate ... Water is usually treated with 0.1% v/v DEPC for at least 2 hours at 37 °C and then autoclaved ...
tert-Butyl alcohol is the simplest tertiary alcohol, with a formula of (CH 3) 3 COH (sometimes represented as t-BuOH). Its isomers are 1-butanol , isobutanol , and butan-2-ol . tert -Butyl alcohol is a colorless solid, which melts near room temperature and has a camphor -like odor.
An important example is di-tert-butyl tricarbonate (H 3 C−) 3 C−C 3 O 7 −C(−CH 3) 3, an intermediate in the synthesis of di-tert-butyl dicarbonate. [1] The term tricarbonate is sometimes used for salts that contain three carbonate dianions in their covalent structure or stoichiometric formula, such as cerium tricarbonate Ce 2 (CO 3) 3.
tert-Butyl acetate, t-butyl acetate or TBAc is a colorless flammable liquid with a camphor- or blueberry-like smell. It is used as a solvent in the production of lacquers, enamels, inks, adhesives, thinners and industrial cleaners.
2,4-Dimethyl-6-tert-butylphenol is the organic compound with the formula Me 2 (tert-Bu)C 6 H 2 OH (Me = methyl, tert-Bu = tertiary butyl). It is a colorless oil that is classified as an alkylated phenol .