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Specific volumes of pure ammonia under the pressure corresponding to saturation have been determined from -78° to 100° C. The method employed is similar to one previously used by Dieterici, and consists essentially in observing, at various temperatures, the volumes of the liquid and vapour phases in equilibrium in a closed vessel.
The Kjeldahl method or Kjeldahl digestion (Danish pronunciation: [ˈkʰelˌtɛˀl]) in analytical chemistry is a method for the quantitative determination of a sample's organic nitrogen plus ammonia/ammonium (NH 3 /NH 4 +). Without modification, other forms of inorganic nitrogen, for instance nitrate, are not included in this measurement.
Ammonia: inorganic; the precursor to most nitrogen-containing compounds; used to make fertilizer Ammonium hydroxide: aqueous ammonia; used in traditional qualitative inorganic analysis: Azobisisobutyronitrile: organic compound; often used as a foamer in plastics and rubber and as a radical initiator: Baeyer's reagent
Chemical ionization can also be used to identify and quantify an analyte present in a sample, by coupling chromatographic separation techniques to CI [3] such as gas chromatography (GC), high performance liquid chromatography (HPLC) and capillary electrophoresis (CE). This allows selective ionization of an analyte from a mixture of compounds ...
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Classical qualitative inorganic analysis is a method of analytical chemistry which seeks to find the elemental composition of inorganic compounds.It is mainly focused on detecting ions in an aqueous solution, therefore materials in other forms may need to be brought to this state before using standard methods.
In these methods, a fixed volume with a known excess amount of the oxidant is added to a sample of the solution being analyzed. After a refluxing digestion step, the initial concentration of organic substances in the sample is calculated from a titrimetric or spectrophotometric determination of the oxidant remaining in the sample.
Ammonia reacts with Berthelot's reagent to form a blue product which is used in a colorimetric method for determining ammonia. The reagent can also be used for determining urea. In this case the enzyme urease is used to catalyze the hydrolysis of urea into carbon dioxide and ammonia. The ammonia is then determined with Berthelot's reagent.