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Sodium methoxide is prepared by treating methanol with sodium: 2 Na + 2 CH 3 OH → 2 CH 3 ONa + H 2. The reaction is so exothermic that ignition is possible. The resulting solution, which is colorless, is often used as a source of sodium methoxide, but the pure material can be isolated by evaporation followed by heating to remove residual methanol.
Potassium methoxide is a white to yellowish, hygroscopic, odorless crystalline powder which reacts violently with water forming potassium hydroxide and methanol. The aqueous solutions obtained are highly basic and have a corrosive effect. The substance is classified as an inflammable solid with a spontaneous ignition temperature of 70 °C. [6]
Methanol and its vapours are flammable. Moderately toxic for small animals – Highly toxic to large animals and humans (in high concentrations) – May be fatal/lethal or cause blindness and damage to the liver, kidneys, and heart if swallowed – Toxicity effects from repeated over exposure have an accumulative effect on the central nervous system, especially the optic nerve – Symptoms may ...
Electrolytes used for electropolishing are most often concentrated acid solutions such as mixtures of sulfuric acid and phosphoric acid. Other electropolishing electrolytes reported in the literature include mixtures of perchloric acid with acetic anhydride (which has caused fatal explosions), and methanolic solutions of sulfuric acid. [3]
The complex is prepared by treating an aqueous methanolic solution of hydrated rhodium trichloride with ethylene at room temperature. Rh(III) is reduced with oxidation of ethylene to acetaldehyde: 2 RhCl 3 (H 2 O) 3 + 6 C 2 H 4 → Rh 2 Cl 2 (C 2 H 4) 4 + 2 CH 3 CHO + 4 HCl + 4 H 2 O
Benzyltrimethylammonium hydroxide, also known as Triton B or trimethylbenzylammonium hydroxide, is a quaternary ammonium salt that functions as an organic base. It is usually handled as a solution in water or methanol.
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Illustrative is the preparation of tetramethylammonium fluoride: [6] NMe 4 + OH − + HF → NMe 4 + F − + H 2 O. Solutions of TMAH may be used to make other tetramethylammonium salts in metathesis reactions with ammonium (NH 4 +) salts. For example, tetramethylammonium thiocyanate may be prepared from ammonium thiocyanate as follows: [7]