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A centrifugal evaporator often comprises a vacuum pump connected to a centrifuge chamber in which the samples are placed. Many systems also have a cold trap or solvent condenser placed in line between the vacuum pump and the centrifuge chamber to collect the evaporated solvents. The most efficient systems also have a cold trap on the pump exhaust.
Single-stage vacuum pumps typically produce vacuum to 35 torr (mm Hg) or 47 millibars (4.7 kPa), and two-stage pumps can produce vacuum to 25 torr, assuming air is being pumped and the ring-liquid is water at 15 °C (59 °F) or less. Dry air and 15 °C sealant-water temperature is the standard performance basis, which most manufacturers use for ...
Cleaning methods encompass solvent cleaning, hot alkaline detergent cleaning, electro-cleaning, and acid etch. In industrial settings, the water-break test is a common practice to assess machinery cleanliness. This test involves thoroughly rinsing and vertically holding the surface.
Pumps that use oil either as their working fluid (diffusion pumps), or as their lubricant (mechanical rotary pumps), are often the sources of contamination in vacuum systems. Placing a cold trap at the mouth of such a pump greatly lowers the risk that oil vapours will backstream into the cavity.
Pump size is also determined by the depth and weight of the oil to remove, with deeper extraction requiring more power to move the increased weight of the discharge column (discharge head). A beam-type pumpjack converts the rotary motion of the motor (usually an electric motor ) to the vertical reciprocating motion necessary to drive the ...
Mixer-settler scheme. Mixer settlers are a class of mineral process equipment used in the solvent extraction process. A mixer settler consists of a first stage that mixes the phases together followed by a quiescent settling stage that allows the phases to separate by gravity.
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