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Tetrahydrofuran (THF), or oxolane, is an organic compound with the formula (CH 2) 4 O. The compound is classified as heterocyclic compound , specifically a cyclic ether . It is a colorless, water- miscible organic liquid with low viscosity .
Phase behavior Triple point: 164.76 K (−108.39 °C), ? Pa Critical point: 541 K (268 °C), 5190 kPa Std enthalpy change of fusion, Δ fus H o: 8.540 kJ/mol Std entropy change
It is produced by polymerization of tetrahydrofuran as well as 1,4-butanediol. The product is commercially available as polymers of low average molecular weights, between 250 and 3000 daltons. In this form it is a white waxy solid that melts between 20 and 30 °C.
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tetrahydrofuran: 109-99-9 C 6 H 14 O 4: triethylene glycol: 112-27-6 Inorganic compounds. Chemical formula Name CAS number N 2 H 4: hydrazine: 302-01-2 HNO 3: nitric ...
For example, tetrahydrofuran-3-one (3-ketotetrahydrofuran) [12] and 3-aminotetrahydrofuran [13] have been synthesized from 3-hydroxytetrahydrofuran and used in pharmaceutical syntheses. Additionally, additive amounts (0.05-0.15 weight %) of the nitrate ester manufactured by sulfuric acid - nitric acid nitration of 3-hydoxytetrahydrofuran have ...
Deuterated tetrahydrofuran (d 8-THF) is a colourless, organic liquid at standard temperature and pressure. [1] This heterocyclic compound has the chemical formula C 4 D 8 O, and is an isotopologue of tetrahydrofuran. [2] Deuterated THF is used as a solvent in NMR spectroscopy, though its expense can often be prohibitive. [citation needed]
The order of addition of the reagents of the Mitsunobu reaction can be important. Typically, one dissolves the alcohol, the carboxylic acid, and triphenylphosphine in tetrahydrofuran or other suitable solvent (e.g. diethyl ether), cool to 0 °C using an ice-bath, slowly add the DEAD dissolved in THF, then stir at room temperature for several hours.
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