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A duoplasmatron is a type of glow discharge ion source that consists of a hot cathode or cold cathode that produces a plasma that is used to ionize a gas. [1] [22] THey can produce positive or negative ions. [23] They are used for secondary ion mass spectrometry, ion beam etching, and high-energy physics. [24] [25] [26]
A mass spectrometer consists of three components: an ion source, a mass analyzer, and a detector. The ionizer converts a portion of the sample into ions. There is a wide variety of ionization techniques, depending on the phase (solid, liquid, gas) of the sample and the efficiency of various ionization mechanisms for the unknown species.
In mass spectrometry, direct analysis in real time (DART) is an ion source that produces electronically or vibronically excited-state species from gases such as helium, argon, or nitrogen that ionize atmospheric molecules or dopant molecules. The ions generated from atmospheric or dopant molecules undergo ion-molecule reactions with the sample ...
A constant current of 2–5 microamps is maintained from the corona needle. Sample ions are produced by ion-molecule reactions (as described below), and pass through a small orifice or tube into the ion transfer region leading to the mass spectrometer. Various geometries of ion source are possible, depending on application.
Meanwhile, photoionization has been used for GC detection and as a source for ion mobility spectrometry for many years suggesting the potential for use in mass spectrometry. [13] The first development of APPI for LC/MS was reported by Robb, Covey, and Bruins [14] and by Syage, Evans, and Hanold in 2000. [15]
A schematic diagram of chemical ionization source. Chemical ionization (CI) is a soft ionization technique used in mass spectrometry. [1] [2] This was first introduced by Burnaby Munson and Frank H. Field in 1966. [3] This technique is a branch of gaseous ion-molecule chemistry. [2]
The first stage of the instrument is an ion source where samples are converted to gas phase ions. Many ionization methods similar to those traditionally used for mass spectrometry have been employed for IM-MS depending on the physical state of the analyte. [9]
Schematic of a fast atom bombardment ion source for a mass spectrometer. Fast atom bombardment (FAB) is an ionization technique used in mass spectrometry in which a beam of high energy atoms strikes a surface to create ions. [1] [2] [3] It was developed by Michael Barber at the University of Manchester in 1980. [4]
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