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The Dumas method of molecular weight determination was historically a procedure used to determine the molecular weight of an unknown volatile substance. [ 1 ] [ 2 ] The method was designed by the French chemist Jean Baptiste André Dumas , after whom the procedure is now named.
The Siwoloboff method is used to determine the boiling point of small samples of liquid chemicals. A sample in an ignition tube (also called a fusion tube) is attached to a thermometer with a rubber band, and immersed in a Thiele tube, water bath, or other suitable medium for heating. A sealed capillary, open end pointing down, is placed in the ...
Using the water bath technique for low-acid foods (foods with pH greater than 4.6). [15] Otherwise correct water bath or pressure canning but processing for too little time, the wrong pressure, or not considering variations in time/pressure due to altitude. Re-using one-use seals; Using cracked or chipped jars
A sealed capillary, open end pointing down, is placed in the fusion tube. The Thiele tube is heated; dissolved gases evolve from the sample first. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample.
A water bath is laboratory equipment made from a container filled with heated water. It is used to incubate samples in water at a constant temperature over a long period of time. Most water baths have a digital or an analogue interface to allow users to set a desired temperature, but some water baths have their temperature controlled by a ...
In physics, an ebullioscope (from Latin ēbullīre 'to boil') is an instrument for measuring the boiling point of a liquid. This can be used for determining the alcoholic strength of a mixture, or for determining the molecular weight of a non-volatile solute based on the boiling-point elevation. The procedure is known as ebullioscopy.
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This page contains tables of azeotrope data for various binary and ternary mixtures of solvents. The data include the composition of a mixture by weight (in binary azeotropes, when only one fraction is given, it is the fraction of the second component), the boiling point (b.p.) of a component, the boiling point of a mixture, and the specific gravity of the mixture.