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Septa seal the two conical flasks. A cannula is used to transfer THF from the flask on the right to the flask on the left.. Cannula transfer or cannulation is a set of air-free techniques used with a Schlenk line, in transferring liquid or solution samples between reaction vessels via cannulae, avoiding atmospheric contamination.
cannula transfer, where liquids or solutions of air-sensitive reagents are transferred between different vessels stoppered with septa using a long thin tube known as a cannula. Liquid flow is achieved via vacuum or inert gas pressure. [3] A cannula is used to transfer THF from the flask on the right to the flask on the left.
the use of syringes and rubber septa to transfer liquids and solutions; [6] cannula transfer, where liquids or solutions of air-sensitive reagents are transferred between different vessels stoppered with septa using a long thin tube known as a cannula. Liquid flow is supported by vacuum or inert-gas pressure.
A Schlenk flask, or Schlenk tube, is a reaction vessel typically used in air-sensitive chemistry, invented by Wilhelm Schlenk.It has a side arm fitted with a PTFE or ground glass stopcock, which allows the vessel to be evacuated or filled with gases (usually inert gases like nitrogen or argon).
Crude versions of conically tapered ground glass joints have been made for quite a while, [1] particularly for stoppers for glass bottles and retorts. [2] Crude glass joints could still be made to seal well by grinding the two parts of a joint against each other using an abrasive grit, but this led to variations between joints and they would not seal well if mated to a different joint.
It is often necessary to maintain the Büchner flask and, incidentally, the vacuum flask. The rigidity of the vacuum pipes and the difference in height between the different parts of the apparatus (as visible in the diagram) make such an apparatus relatively unstable. Therefore, a three-pronged clamp should be used to maintain the Büchner flask.
A gas syringe has an inner syringe chamber which has a ground glass surface. The syringe barrel also has a ground glass surface. The ground surface of the barrel moves freely within the ground glass surface of the syringe chamber with very little friction. The close mating of these ground glass surfaces also gives a reasonably gas-tight seal. [3]
It is often used in combination with a Büchner flask, Büchner ring and sinter seals. A vacuum tight seal and stability of the Büchner flask and filter are essential during the filtration process. A Büchner ring can be used with Büchner funnels, flasks, glass crucibles and Gooch crucibles. The wide flange and large surface contact ensures ...