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It may be prepared via the Schiemann reaction, in which a 4-aminobenzoic acid, protected as the ethyl ester, is diazotised and then fluoride introduced using tetrafluoroborate. Hydrolysis of the ester converts it back to the free acid. [2] 4-Fluorobenzoic acid has been observed to form by the aerobic biotransformation of 4-fluorocinnamic acid. [3]
Fluorobenzoic acid may refer to: 2-Fluorobenzoic acid (ortho) 3-Fluorobenzoic acid (meta) 4-Fluorobenzoic acid (para) This page was last edited on 9 ...
Pages in category "4-Fluorophenyl compounds" The following 200 pages are in this category, out of approximately 203 total. This list may not reflect recent changes .
The traditional Balz–Schiemann reaction employs HBF 4 and involves isolation of the diazonium salt. Both aspects can be profitably modified. Other counterions have been used in place of tetrafluoroborates, such as hexafluorophosphates (PF 6 −) and hexafluoroantimonates (SbF 6 −) with improved yields for some substrates.
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Fluorobenzoic acids. 2-Fluorobenzoic acid; 3-Fluorobenzoic acid; 4-Fluorobenzoic acid This page was last edited on 28 August 2022, at 12:42 ...
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Pentafluorobenzoic acid is prepared by treating pentafluorophenyllithium (or pentafluorophenyl Grignard reagent) with carbon dioxide. These reagents are usually prepared in situ from pentafluorobenzene and bromopentafluorobenzene. [1] [2] It arises via the reaction of perfluorotoluene with trifluoroacetic acid and antimony pentafluoride. [3]