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The oil level is a little low now to compensate for expansion when heating commences. The Thiele tube, named after the German chemist Johannes Thiele, is a laboratory glassware designed to contain and heat an oil bath. Such a setup is commonly used in the determination of the melting point or boiling point of a substance.
The sample is then heated, either by a heating block or an oil bath, and as the temperature increases, the sample is observed to determine when the phase change from solid to liquid occurs. The operator of the apparatus records the temperature range starting with the initial phase-change temperature and ending with the completed phase-change ...
The apparatus is heated. Dissolved gases evolve from the sample first, and the air in the capillary tube expands. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample. [1] [2] [3] [4]
A pressure cooker is a sealed vessel for cooking food with the use of high pressure steam and water or a water-based liquid, a process called pressure cooking. The high pressure limits boiling and creates higher temperatures not possible at lower pressures, allowing food to be cooked faster than at normal pressure.
A bain-marie (English: / ˌ b æ n m ə ˈ r iː / BAN-mə-REE, French: [bɛ̃ maʁi]), also known as a water bath or double boiler, a type of heated bath, is a piece of equipment used in science, industry, and cooking to heat materials gently or to keep materials warm over a period of time. A bain-marie is also used to melt ingredients for ...
A process of heating oil shale to produce shale oil, oil shale gas, and spent shale is commonly called retorting. Airtight vessels to apply pressure as well as heat are called autoclaves . In the food industry , pressure cookers are often referred to as "retorts", meaning " canning retorts" for sterilization under high temperature (116–130 °C).
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
In order for a substance to condense from a pure vapor, the pressure of the latter must be higher than the vapor pressure of the adjacent liquid; that is, the liquid must be below its boiling point at that pressure. In most designs, the liquid is only a thin film on the inner surface of the condenser, so its temperature is essentially the same ...
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