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Boiling chips. A boiling chip, boiling stone, or porous bit anti-bumping granule is a tiny, unevenly shaped piece of substance added to liquids to make them boil more calmly. Boiling chips are frequently employed in distillation and heating. When a liquid becomes superheated, a speck of dust or a stirring rod can cause violent flash boiling.
Boiling chips are added in distilling flasks for distillations or boiling chemical reactions to allow a nucleation site for gradual boiling. This nucleation avoids a sudden boiling surge where the contents may overflow from the boiling flask. Stirring bars or other stirring devices suited for round-bottom flasks are sometimes used. [4]
The most common way of preventing bumping is by adding one or two boiling chips to the reaction vessel. However, these alone may not prevent bumping and for this reason it is advisable to boil liquids in a boiling tube, a boiling flask, or an Erlenmeyer flask. In addition, heating test tubes should never be pointed towards any person, just in ...
In the vacuum apparatus here, it distills off into the connected receiver flask on the left at only 70 °C. Vacuum distillation or distillation under reduced pressure is a type of distillation performed under reduced pressure, which allows the purification of compounds not readily distilled at ambient pressures or simply to save time or energy.
Volumetric flask is used for preparing liquids with volumes of high precision. It is a flask with an approximately pear-shaped body and a long neck with a circumferential fill line. Dewar flask is a double-walled flask having a near-vacuum between the two walls. These come in a variety of shapes and sizes; some are large and tube-like, others ...
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
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