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A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
After many cycles the desired compound is concentrated in the distillation flask. The advantage of this system is that instead of many portions of warm solvent being passed through the sample, just one batch of solvent is recycled. After extraction the solvent is removed, typically by means of a rotary evaporator, yielding the extracted ...
Rotary evaporators use a vacuum pump to create a low pressure over a solvent while simultaneously rotating the liquid flask to increase surface area and decrease bubble size. Typically, the vapor is passed over a cold finger or coil so that the vaporized material does not damage the pump.
Organic solvent or salt Temp (°C) Dry ice p-xylene +13 Dry ice Dioxane +12 Dry ice Cyclohexane +6 Dry ice Benzene +5 Dry ice Formamide +2 Ice Salts (see: left) 0 to −40 Liquid N 2: Cycloheptane −12 Dry ice Benzyl alcohol −15 Dry ice Tetrachloroethylene −22 Dry ice Carbon tetrachloride −23 Dry ice 1,3-Dichlorobenzene −25 Dry ice o ...
Centrifugal evaporator patent from 1875. A centrifugal evaporator is a device used in chemical and biochemical laboratories for the efficient and gentle evaporation of solvents from many samples at the same time, and samples contained in microtitre plates. If only one sample required evaporation then a rotary evaporator is most often
The best way to achieve high economies (which can be well over 100%) is to use multiple effect evaporator, whereby the vapour from one evaporator – or effect – is used to heat the feed in the next effect, where boiling occurs at lower pressure and temperature [3] Thermo-compression of the vapour, whereby the vapour will condense at a ...
A Kugelrohr (German for "ball tube") is a short-path vacuum distillation apparatus [1]: 150 typically used to distill relatively small amounts of compounds with high boiling points (usually greater than 300 °C) under greatly reduced pressure.
The handling of this chemical may incur notable safety precautions. It is highly recommend that you seek the Material Safety Datasheet ( MSDS ) for this chemical from a reliable source such as eChemPortal , and follow its directions.