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Calibration involves taking three readings: one with an empty tube R 0, one with a tube filled with the calibration reference material, and one with the tube filled with the sample R s. Some balances feature an auto-tare function that eliminates the need for the R 0 measurement. [11] The first two readings provide a calibration constant (C).
Schematic diagram of Gouy balance. The Gouy balance, invented by the French physicist Louis Georges Gouy, is a device for measuring the magnetic susceptibility of a sample. . The Gouy balance operates on magnetic torque, by placing the sample on a horizontal arm or beam suspended by a thin fiber, and placing either a permanent magnet or electromagnet on the other end of the arm, there is a ...
The current is proportional to the magnetization of the sample - the greater the induced current, the greater the magnetization. As a result, typically a hysteresis curve will be recorded [5] and from there the magnetic properties of the sample can be deduced. The idea of vibrating sample came from D. O. Smith's [6] vibrating-coil magnetometer.
However, magnetic torque magnetometry doesn't measure magnetism directly as all the previously mentioned methods do. Magnetic torque magnetometry instead measures the torque τ acting on a sample's magnetic moment μ as a result of a uniform magnetic field B, τ = μ × B. A torque is thus a measure of the sample's magnetic or shape anisotropy.
A popular pulsed EPR experiments currently is double electron-electron resonance (DEER), which is also known as pulsed electron-electron double resonance (PELDOR). [5] In this experiment, two frequencies control two spins to probe their coupling. The distance between the spins can then be inferred from their coupling strength.
This section gives an example for an experiment carried out by Strick, Allemand, Croquette [9] with the help of magnetic tweezers. A double-stranded DNA molecule is fixed with multiple binding sites on one end to a glass surface and on the other to a magnetic micro bead, which can be manipulated in a magnetic tweezers apparatus.
These methods employ a pump-probe setup. In most cases the pump and probe are both generated by a pulsed laser and in the UV region. The pump excites the atom or molecule of interest, and the probe ionizes it. The electrons or positive ions resulting from this event are then detected. As the time delay between the pump and the probe are changed ...
Solid-state 900 MHz (21.1 T [1]) NMR spectrometer at the Canadian National Ultrahigh-field NMR Facility for Solids. Solid-state nuclear magnetic resonance (ssNMR) is a spectroscopy technique used to characterize atomic-level structure and dynamics in solid materials. ssNMR spectra are broader due to nuclear spin interactions which can be categorized as dipolar coupling, chemical shielding ...