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Cathodic reduction of graphite perchlorate is analogous to heating KC 8, which leads to a sequential elimination of HClO 4. Both graphite bisulfate and graphite perchlorate are better conductors as compared to graphite, as predicted by using a positive-hole mechanism. [4] Reaction of graphite with [O 2] + [AsF 6] − affords the salt [C 8 ...
The HIP process subjects a component to both elevated temperature and isostatic gas pressure within a high-pressure containment vessel, unlike the cold isostatic pressing (CIP), where the component is maintained at room temperature. [1] The pressurizing gas most widely used is argon. An inert gas is used so that the material does not chemically ...
More conveniently, the salt can be made by reacting nitric acid with aluminium hydroxide. Aluminium nitrate may also be prepared a metathesis reaction between aluminium sulfate and a nitrate salt with a suitable cation such as barium, strontium, calcium, silver, or lead. e.g. Al 2 (SO 4) 3 + 3 Ba(NO 3) 2 → 2 Al(NO 3) 3 + 3 BaSO 4.
Similar reactions occur with other protic reagents: [1] Al 4 C 3 + 12 HCl → 4 AlCl 3 + 3 CH 4 Reactive hot isostatic pressing (hipping) at ≈40 MPa of the appropriate mixtures of Ti, Al 4 C 3 graphite, for 15 hours at 1300 °C yields predominantly single-phase samples of Ti 2 AlC 0.5 N 0.5 , 30 hours at 1300 °C yields predominantly single ...
Treating graphite with strong acids in the presence of oxidizing agents causes the graphite to oxidise. Graphite bisulfate, [C 24] + [HSO 4] −, is prepared by this approach using sulfuric acid and a little nitric acid or chromic acid. The analogous graphite perchlorate can be made similarly by reaction with perchloric acid. [clarification needed]
The expanded graphite can be used to make graphite foil or used directly as a "hot top" compound to insulate molten metal in a ladle or red-hot steel ingots and decrease heat loss, or as firestops fitted around a fire door or in sheet metal collars surrounding plastic pipe (during a fire, the graphite expands and chars to resist fire ...
Isostatic pressing is the process where casting are pressed into compact solids using a mould and pressure. Eletrophoretic deposition is the process where migrating colloidal particles suspended in a medium using an electrical field to get the desired material.
An electric current is passed through the graphite rods which heats the mixture to 1700–2500 °C. [1] The result of the carbothermic reaction is a layer of silicon carbide (especially in its alpha and beta phases) [1] forming around the rod and emission of carbon monoxide (CO). There are four chemical reactions in the production of silicon ...