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4-Bromobenzaldehyde, or p-bromobenzaldehyde, is an organobromine compound with the formula BrC 6 H 4 CHO. It is one of three isomers of bromobenzaldehyde . [ 3 ] It displays reactivity characteristic of benzaldehyde and an aryl bromide .
The complete removal of the water is critical for the reaction conversion, due to the pronounced hygroscopy of potassium hydroxide, which contains about 10% of water. [3] The significantly higher dissolution rate of potassium hydroxide in methanol compared to sodium hydroxide is advantageous.
Methyl benzoate is an organic compound. It is an ester with the chemical formula C 6 H 5 COOCH 3 , sometimes abbreviated as PhCO 2 Me , where Ph and Me are phenyl and methyl , respectively. Its structure is C 6 H 5 −C(=O)−O−CH 3 .
Potassium benzoate (E212), the potassium salt of benzoic acid, is a food preservative that inhibits the growth of mold, yeast and some bacteria. It works best in low- pH products, below 4.5, where it exists as benzoic acid.
These solutions are identified by CAS number 75-59-2. Several hydrates such as N(CH 3) 4 OH·xH 2 O. have been crystallized. [3] These salts contain well separated Me 4 N + cations and hydroxide anions (Me is an abbreviation of methyl group). The hydroxide groups are linked by hydrogen bonds to the water of crystallization. Anhydrous TMAH has ...
Benzyl bromide is used in organic synthesis for the introduction of the benzyl groups when the less expensive benzyl chloride is insufficiently reactive. [6] [7] Benzylations are often achieved in the presence of catalytic amounts of sodium iodide, which generates the more reactive benzyl iodide in situ. [3]
Tolyltriazole is a mixture of isomers or congeners that differ from benzotriazole by the addition of one methyl group attached somewhere on the benzene ring. "The term tolyltriazole (CAS 29385-43-1) generally [refers to] the commercial mixture composed of approximately equal amounts of 4- and 5-methylbenzotriazole, with small quantities of [their respective 7- and 6-methyl tautomers]".
One variant of the reaction involves iminodiacetonitrile or iminodiacetic acid (step 1'), which reacts in a weakly acidic medium (pH 6) with hydrogen cyanide and ethanal to form methylglycinonitrile-N,N-diacetic acid, the nitrile group of which is hydrolyzed with sodium hydroxide to trisodium N-(1-carboxylatoethyl)iminodiacetate (step 2').