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A fractionating column or fractional column is equipment used in the distillation of liquid mixtures to separate the mixture into its component parts, or fractions, based on their differences in volatility. Fractionating columns are used in small-scale laboratory distillations as well as large-scale industrial distillations.
In 1943 Dr Olaf George Dixon of ICI applied for a patent of a new product for column distillation. [1] He used stainless steel mesh instead of sheet steel in the Lessing ring in order to improve the pressure drop of the packed column (in fact, they were called "wire gauze Lessing rings" in a 1949 publication [2]).
Distillation by column still is the traditional method for production of Armagnac, although distillation by pot still is allowed. The use of column stills for the distillation of Cognac is forbidden, although they may be used for other types of brandy , likewise malt Scotch Whiskies must be distilled in a pot still.
The crude oil is fed to a stabilizer which is typically a tray or packed tower column that achieves a partial fractionation or distillation of the oil. [4] The heavier components, pentane (C 5 H 12 ), hexane (C 6 H 14 ), and higher hydrocarbons (C 7 +), flow as liquid down through the column where the temperature is increasingly higher.
Distillation, also classical distillation, is the process of separating the component substances of a liquid mixture of two or more chemically discrete substances; the separation process is realized by way of the selective boiling of the mixture and the condensation of the vapors in a still.
Image 1: Typical industrial distillation towers Image 2: A crude oil vacuum distillation column as used in oil refineries. Continuous distillation, a form of distillation, is an ongoing separation in which a mixture is continuously (without interruption) fed into the process and separated fractions are removed continuously as output streams.
The concept of theoretical plates in designing distillation processes has been discussed in many reference texts. [2] [3] Any physical device that provides good contact between the vapor and liquid phases present in industrial-scale distillation columns or laboratory-scale glassware distillation columns constitutes a "plate" or "tray". Since an ...
Schematics of a plate column with bubble cap trays. The feed to the column can be liquid, gas or gas and liquid at equilibrium. Inside the column there are always two phases: one gas phase and one liquid phase. The liquid phase flows downward through the column via gravity, [1] while the gas phase flows upward.
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