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An example of back titration, the Volhard method, named after Jacob Volhard, involves the addition of excess silver nitrate to the analyte; the silver chloride is filtered, and the remaining silver nitrate is titrated against ammonium thiocyanate, [1] with ferric ammonium sulfate as an indicator which forms blood-red [Fe(OH 2) 5 (SCN)] 2+ at the end point:
A chloridometer is a measuring instrument used to determine the concentration of chloride ions (Cl –) in a solution.It uses a process known as coulometric titration or amperostatic coulometry, the accepted electrochemistry reference method to determine the concentration of chloride in biological fluids, including blood serum, blood plasma, urine, sweat, and cerebrospinal fluid.
The precipitation of the strongly coloured silver chromate is used to indicate the endpoint in the titration of chloride with silver nitrate in the Mohr method of argentometry. Example of Mohr argentometric titration near the endpoint: note the characteristic brick-red colour appearing due to silver chromate formation. The reactivity of the ...
Cerimetry or cerimetric titration, also known as cerate oximetry, is a method of volumetric chemical analysis developed by Ion Atanasiu. It is a redox titration in which an iron(II)–1,10-phenanthroline complex color change indicates the end point. Ferroin can be reversibly discolored in its oxidized form upon titration with a Ce 4+ solution ...
A Westphal balance (also known as a Mohr balance) is a scientific instrument used to measure the density of liquids. [1] [2] [3] References
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This technique was a standard method for the determination of chloride ions in laboratories worldwide. The method involves the addition of mercury thiocyanate to a solution with an unknown concentration of chloride ions and iron as a reagent. The chloride ions cause the mercury thiocyanate salt to dissociate and the thiocyanate ion to bind Fe ...
Classical qualitative inorganic analysis is a method of analytical chemistry which seeks to find the elemental composition of inorganic compounds. It is mainly focused on detecting ions in an aqueous solution , therefore materials in other forms may need to be brought to this state before using standard methods.