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Steam distillation is a separation process that consists of distilling water together with other volatile and non-volatile components. The steam from the boiling water carries the vapor of the volatiles to a condenser ; both are cooled and return to the liquid or solid state, while the non-volatile residues remain behind in the boiling container.
Steam from boiling water is passed through the raw material for 60–105 minutes, which drives out most of their volatile fragrant compounds. The condensate from distillation, which contain both water and the aromatics, is settled in a Florentine flask. This allows for the easy separation of the fragrant oils from the water as the oil will ...
Florentine flask Florentine flask. A florentine flask, also known as florentine receiver, florentine separator or essencier (from the French), other shapes called florentine vase or florentine vessel, is an oil–water separator fed with condensed vapors of a steam distillation in a fragrance extraction process.
Like vacuum distillation, steam distillation is a method for distilling compounds which are heat-sensitive. [1]: 151–153 The temperature of the steam is easier to control than the surface of a heating element and allows a high rate of heat transfer without heating at a very high temperature. This process involves bubbling steam through a ...
The science of distillation is based on the fact that different substances evaporate at different temperatures. Unlike other extraction techniques based on solubility of a compound in either water or oil, distillation will separate components regardless of their solubility. The distillate will contain compounds that vaporize at or below the ...
This equipment can be used in cases other than simple removal of water. One example is the esterification of butanol with acetic acid catalyzed by sulfuric acid. The vapor contains 63% ester, 29% water and 8% alcohol at reflux temperature and the organic layer in the trap contains 86% ester, 11% alcohol and 3% water which is reintroduced.
This new continuous distillation method produced whisky much more efficiently than the traditional pot stills, [14] without the need for cleaning after each batch was made. [ 15 ] As the reciprocating steam engines of the time were unable to feed the still with the necessary high temperature/pressure steam, it took some time for the Coffey ...
Steam is also frequently used as a stripping agent for water treatment. Volatile organic compounds are partially soluble in water and because of environmental considerations and regulations, must be removed from groundwater, surface water, and wastewater. [5] These compounds can be present because of industrial, agricultural, and commercial ...
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