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16th century cupellation furnaces (per Agricola). Cupellation is a refining process in metallurgy in which ores or alloyed metals are treated under very high temperatures and subjected to controlled operations to separate noble metals, like gold and silver, from base metals, like lead, copper, zinc, arsenic, antimony, or bismuth, present in the ore.
Crucibles used in Czochralski method Melting gold in a graphite crucible Three crucibles used by Thomas Edison. Crucibles are used in the laboratory to contain chemical compounds when they are heated to extremely high temperatures. Crucibles are available in several sizes and typically come with a correspondingly-sized lid. [20]
The process can be carried out in a horizontal or vertical orientation, and usually involves a rotating crucible/ampoule to stir the melt. [ 1 ] The Bridgman method is a popular way of producing certain semiconductor crystals such as gallium arsenide , for which the Czochralski method is more difficult.
When silicon is grown by the Czochralski method, the melt is contained in a silica crucible. During growth, the walls of the crucible dissolve into the melt and Czochralski silicon therefore contains oxygen at a typical concentration of 10 18 cm −3. Oxygen impurities can have beneficial or detrimental effects.
One process for X-ray fluorescence assay involves melting the material in a furnace and stirring to make a homogeneous mix. Following this, a sample is taken from the centre of the molten sample. Samples are typically taken using a vacuum pin tube. [4] The sample is then tested by X-ray fluorescence spectroscopy. Metallurgical assay is ...
This cylinder, referred to as an electrode is then put into a large cylindrical enclosed crucible and brought to a metallurgical vacuum (0.001–0.1 mmHg or 0.1–13.3 Pa). At the bottom of the crucible is a small amount of the alloy to be remelted, which the top electrode is brought close to prior to starting the melt.
Crucible Industries, commonly known as Crucible, is an American company which develops and manufactures specialty steels, and is the sole producer of a line of sintered steels known as Crucible Particle Metallurgy (CPM) steels.
First, the gold-silver ore is melted down in the crucible, but with an excess amount of lead. The intense heat then oxidizes the lead which reacts quickly and binds with the impurities in the gold-silver ore. Since both gold and silver have low reactivity with the impurities, they remain behind once the slag is removed. The last stage involves ...
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