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A sublimatory [1] [2] or sublimation apparatus is equipment, commonly laboratory glassware, for purification of compounds by selective sublimation. In principle, the operation resembles purification by distillation , except that the products do not pass through a liquid phase .
An ordinary glovebox, showing the two gloves for manipulation, with airlock on the right. The most straightforward type of air-free technique is the use of a glovebox.A "glove bag" uses the same idea, but is usually a poorer substitute because it is more difficult to purge, and less well sealed.
The Knudsen cell is used to measure the vapor pressures of a solid with very low vapor pressure. Such a solid forms a vapor at low pressure by sublimation.The vapor slowly effuses through the pinhole, and the loss of mass is proportional to the vapor pressure and can be used to determine this pressure. [1]
The term was later also applied to the indirect sublimation transfer printing process, which uses a standard ink-jet printer to deposit sublimation-capable ink onto a transfer sheet. The printed transfer sheet is then pressed with the substrate with heat, transferring the dye to the substrate, such as plastic or fabric, via sublimation.
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The sublimation that occurs at the solid-gas boundary (critical sublimation point) (corresponding to boiling in vaporization) may be called rapid sublimation, and the substance sublimes rapidly. The words "gradual" and "rapid" have acquired special meanings in this context and no longer describe the rate of sublimation. [citation needed]
Sublimation or sublimate may refer to: Sublimation, by Canvas Solaris, 2004; Sublimation (phase transition), directly from the solid to the gas phase; Sublimation (psychology), a mature type of defense mechanism; Sublimate of mercury, or Mercury(II) chloride; Volcanic sublimate, a product of deposition from vapors around volcanic vents