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ZnO creates one of the most diverse range of nanostructures, and there is a great amount of research on different synthesis routes of various ZnO nanostructures. [1] The most common methods to synthesise ZnO structures is using chemical vapor deposition (CVD), which is best used to form nanowires and comb or tree-like structures.
ZnO is a wide-bandgap semiconductor with an energy gap of 3.37 eV at room temperature. [1] ZnO nanoparticles are believed to be one of the three most produced nanomaterials, along with titanium dioxide nanoparticles and silicon dioxide nanoparticles. [2] [3] [4] The most common use of ZnO nanoparticles is in sunscreen.
X-ray crystal truncation rod scattering is a powerful method in surface science, based on analysis of surface X-ray diffraction (SXRD) patterns from a crystalline surface. For an infinite crystal , the diffracted pattern is concentrated in Dirac delta function like Bragg peaks .
X-ray diffraction is a generic term for phenomena associated with changes in the direction of X-ray beams due to interactions with the electrons around atoms. It occurs due to elastic scattering , when there is no change in the energy of the waves.
The Scherrer equation, in X-ray diffraction and crystallography, is a formula that relates the size of sub-micrometre crystallites in a solid to the broadening of a peak in a diffraction pattern. It is often referred to, incorrectly, as a formula for particle size measurement or analysis.
Zinc oxide is an inorganic compound with the formula Zn O.It is a white powder which is insoluble in water. ZnO is used as an additive in numerous materials and products including cosmetics, food supplements, rubbers, plastics, ceramics, glass, cement, lubricants, [12] paints, sunscreens, ointments, adhesives, sealants, pigments, foods, batteries, ferrites, fire retardants, semi conductors ...
An X-ray diffraction pattern of a crystallized enzyme. The pattern of spots (reflections) and the relative strength of each spot (intensities) can be used to determine the structure of the enzyme. The relative intensities of the reflections provides information to determine the arrangement of molecules within the crystal in atomic detail.
WDS has a much finer spectral resolution than EDS. WDS also avoids the problems associated with artifacts in EDS (false peaks, noise from the amplifiers, and microphonics). A high-energy beam of charged particles such as electrons or protons can be used to excite a sample rather than X-rays. This is called particle-induced X-ray emission or PIXE.