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Distillation setup using a retort and tube condenser, from a 1921 book. [5] The simplest type of condenser is a straight tube, cooled only by the surrounding air. The tube is held in a vertical or oblique position, and the vapor is fed through the upper end. The heat of condensation is carried away by convection.
Liebig condenser. The Liebig condenser (/ ˈ l iː b ɪ ɡ /, LEE-big) [1] or straight condenser is a piece of laboratory equipment, specifically a condenser consisting of a straight glass tube surrounded by a water jacket. In typical laboratory operation, such as distillation, the condenser is clamped to a retort stand in vertical
A simple short path vacuum distillation apparatus can be used for bulb-to-bulb distillation. 1: Still pot with stirrer bar/anti-bumping granules 2: Cold finger - Condenser with maximum surface to condense most of the vapour. 3: Cooling water outlet 4: cooling water inlet 5: Vacuum Adapter 6: Receiving Flask.
Distillation was practiced in the ancient Indian subcontinent, which is evident from baked clay retorts and receivers found at Taxila, Shaikhan Dheri, and Charsadda in Pakistan and Rang Mahal in India dating to the early centuries of the Common Era. [17] [18] [19] Frank Raymond Allchin says these terracotta distill tubes were "made to imitate ...
The condenser coil of a refrigerator. In systems involving heat transfer, a condenser is a heat exchanger used to condense a gaseous substance into a liquid state through cooling. In doing so, the latent heat is released by the substance and transferred to the surrounding environment. Condensers are used for efficient heat rejection in many ...
The reflux system in a typical industrial distillation column Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial [ 1 ] and laboratory [ 2 ] distillations .
The lower end of a reflux condenser fits into the top of the cylinder. Immediately below the joint between the condenser and the cylinder is a sloping side-arm that joins the cylinder to a reaction flask. The lower end of the side-arm turns sharply downward, so that the side-arm is connected to the reaction flask by a vertical tube.
They boil the liquid from the bottom of a distillation column to generate vapors which are returned to the column to drive the distillation separation. The heat supplied to the column by the reboiler at the bottom of the column is removed by the condenser at the top of the column. Proper reboiler operation is vital to effective distillation.
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