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Pulse electrolysis is an alternate electrolysis method that utilises a pulsed direct current to initiate non-spontaneous chemical reactions. [1] [2] [3] Also known as pulsed direct current (PDC) electrolysis, the increased number of variables that it introduces to the electrolysis method can change the application of the current to the electrodes and the resulting outcome.
A chemically modified electrode is an electrical conductor that has its surface modified for different electrochemical functions. Chemically modified electrodes are made using advanced approaches to electrode systems by adding a thin film or layer of certain chemicals to change properties of the conductor according to its targeted function.
Chemical modification is the change of biomolecular structure and function due to the addition or removal of modifying elements. [1] This is usually accomplished via chemical reactions or a series of chemical reactions that may or may not be reversible. Chemical modifications can be done to any of the four major macromolecules (proteins ...
Carbon nanotubes and graphene-based materials can be used as electrocatalysts. [27] The carbon surfaces of graphene and carbon nanotubes are well suited to the adsorption of many chemical species, which can promote certain electrocatalytic reactions. [28] In addition, their conductivity means they are good electrode materials. [28]
Potentiometry passively measures the potential of a solution between two electrodes, affecting the solution very little in the process. One electrode is called the reference electrode and has a constant potential, while the other one is an indicator electrode whose potential changes with the sample's composition. Therefore, the difference in ...
The auxiliary electrode may be isolated from the working electrode using a glass frit. Such isolation prevents any byproducts generated at the auxiliary electrode from contaminating the main test solution: for example, if a reduction is being performed at the working electrode in aqueous solution, oxygen may be evolved from the auxiliary electrode.
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A working definition is an electrode that has at least one dimension (the critical dimension) smaller than 25 μm. Platinum electrodes with a radius of 5 μm are commercially available and electrodes with critical dimension of 0.1 μm have been made. Electrodes with even smaller critical dimension have been reported in the literature, but exist ...