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Thermogravimetric analysis or thermal gravimetric analysis (TGA) is a method of thermal analysis in which the mass of a sample is measured over time as the temperature changes. . This measurement provides information about physical phenomena, such as phase transitions, absorption, adsorption and desorption; as well as chemical phenomena including chemisorptions, thermal decomposition, and ...
A diagram which shows the interconnection of process equipment and the instrumentation used to control the process. In the process industry, a standard set of symbols is used to prepare drawings of processes. The instrument symbols used in these drawings are generally based on International Society of Automation (ISA) Standard S5.1
Polymers represent another large area in which thermal analysis finds strong applications. Thermoplastic polymers are commonly found in everyday packaging and household items, but for the analysis of the raw materials, effects of the many additive used (including stabilisers and colours) and fine-tuning of the moulding or extrusion processing used can be achieved by using differential scanning ...
Thermogravimetric Analysis (TGA) may be more useful for decomposition behavior determination. Impurities in polymers can be determined by examining thermograms for anomalous peaks, and plasticisers can be detected at their characteristic boiling points. In addition, examination of minor events in first heat thermal analysis data can be useful ...
Differential thermal analysis (DTA) is a thermoanalytic technique that is similar to differential scanning calorimetry.In DTA, the material under study and an inert reference are made to undergo identical thermal cycles, (i.e., same cooling or heating programme) while recording any temperature difference between sample and reference. [1]
It can do flexure, tensile, and compression testing (even shear and liquid specimens if desired). These analyzers can test higher modulus materials than torsional analyzers. The instrument can do thermomechanical analysis (TMA) studies in addition to the experiments that torsional analyzers can do. Figure 4 shows the general difference between ...
By coupling the thermal analysis instrument, e. g. TGA (thermogravimetry) or DSC (differential scanning calorimetry), with a fast Quadrupole Mass Spectrometer (QMS) the detection of gas separation and identification of the separated components are possible in exact time correlation with the other thermal analysis signals. DSC/TGA-QMS or TGA-QMS ...
A Fisher–Johns apparatus. A melting-point apparatus is a scientific instrument used to determine the melting point of a substance. Some types of melting-point apparatuses include the Thiele tube, Fisher-Johns apparatus, Gallenkamp (Electronic) melting-point apparatus and automatic melting-point apparatus.
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