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The Noack volatility test, named after Kurt Noack, [1] determines the evaporation loss of lubricants in high-temperature service. This test is standardized as ASTM D5800. [2]In this test, a sample is heated at 250 °C for 60 minutes with a constant flow of air over it.
The original Proctor test, ASTM D698 / AASHTO T99, uses a 4-inch-diameter (100 mm) by 4.584-inch-high (116.4 mm) mold which holds 1/30 cubic feet of soil, and calls for compaction of three separate lifts of soil using 25 blows by a 5.5 lb hammer falling 12 inches, for a compactive effort of 12,375 ft-lbf/ft 3.
This method is an improvised version of ASTM D 3612A to do multiple extraction instead of single extraction and based on Toepler principle. In this apparatus a fixed volume of sample oil is directly drawn from a sample tube into a degassing vessel under vacuum, where the gases are released.
The stress intensity factor at the crack tip of a compact tension specimen is [4] = [() / / + / / + /] where is the applied load, is the thickness of the specimen, is the crack length, and is the effective width of the specimen being the distance between the centreline of the holes and the backface of the coupon.
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ASTM D 624 can be applied to measure the resistance to the formation of a tear (tear initiation) and the resistance to the expansion of a tear (tear propagation). Regardless of which of these two is being measured, the sample is held between two holders and a uniform pulling force applied until the aforementioned deformation occurs.
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